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is commonly used The temperature ramp needs to be continued at least 30 C (54 F) above the anticipated transition region The Tg is defined as the temperature at which the two tangent lines for the thermal expansion coefficient intersect Figure 125 shows an example of a typical TMA scan The material has a Tg of 1367 C It is recommended to retest the same sample after allowing it to cool down to room temperature to determine whether the measured value for Tg2 is comparable to the measured value of Tg1 If Tg1 is significantly lower than Tg2, then this could be an indication that the sample material was not fully cured when it was tested the first time If Tg1 is significantly higher than Tg2, that could indicate that the sample material has already started to decompose and was approaching Td.

The authors recommend further testing if these measurements differ by more than 5 C 125212 Tg by Differential Scanning Calorimetry (DSC) Differential scanning calorimetry measures the difference in heat absorption or emission from a test specimen in comparison to a reference sample (usually nitrogen gas)This makes the technique applicable to determine a variety of property changes in polymer materials It can detect the exothermic cure reaction, crystallization energy, and residual reactivity in polymers, as well as endothermic melting points For epoxy-based resin systems, DSC is a well-suited technique as these materials go through a crystalline transition at Tg and this property change can be used to determine the glass transition For other resin systems that are more amorphous and have a Tg that occurs over a wider range (such as polyimides), the detection may be more difficult by DSC than TMA..

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roomed from being hammered into the stack) or do not fit snugly. Tooling pins that do not hold the stack tightly in place or that allow the stack to move create a large variety of problems from burrs and other hole defects to poor registration or drill bit breakage. These unnecessary problems may be prevented by simply replacing tooling pins when they start to show signs of wear or damage. Use tooling pins that are hardened to minimize wear and deformation, and (ideally) 3/16 in in diameter. Pins that are less than 3/16 in in diameter (i.e., 1/8 in) do not hold the stack firmly in place during drilling and may result in stack movement.

Machine variables that affect the drilling process are as follows and as shown in the fishbone diagram of Fig. 24.5.

(i) a dimensional accuracy in the range of some microns (ii) a surface form accuracy in the range of 100 nm or better (iii) a surface texture in the range of 5 nm or better

Drilling machine elements, with major issues and special considerations identi-

Air 24.3.1.1 Quality. Maintaining high levels of air quality is important. Air supplied to the machine and the spindle assemblies needs to be clean and dry. This is accomplished by filters that remove dirt and moisture from the air. In areas where the relative humidity is high, or when using air-bearing-type spindles, an inline air drying and filtering system may be necessary to control air moisture levels and dirt. Moist air causes corrosion of air surfaces (such as the spindle sleeve and other spindle components operating on air) and reduces the life of these components, resulting in increased repair costs. Dirty air affects operation of components relying on air by clogging the channels that supply the air (e.g., to the spindle sleeves and table air shoes). In addition, dirt serves as an abrasive that causes faster wear of machine components, resulting in reduced life cycles between repairs, again increasing downtime and repair costs. Cleaning the machine air filters and purging air compressors and lines on a routine basis may minimize problems resulting from dirt or moisture.

;This code segment code cannot run as it is, it is here as an ;illustration Timer0_int: in save_status, SREG sbi PORTB, 0 ;first put off all LEDs sbi PORTB, 1 ;on PORTB sbi PORTB, 2 sbi PORTB, 3 sbis PORTB, 7 ;this code increments inc count ;count in alternate ISRs cpi count, PLAY_TIME brne still_time ;if play duration is over ldi stat_flag, 0 ;reset the flag still_time: ;see which note to cpi play_t, 0 ;play brne chk2 ldi play_t, T1 out TCNT0, play_t ldi play_t, 0 sbrc stat_flag, 7 ;first check if note is ;being actually played ;if so, cbi PORTB, 0 ;put on LED on PORTB0 rjmp chk5

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